Method for detecting oil content in compressed air
1. Weight method
The gravimetric method refers to the method of determining the analytical results of a certain amount of sample
gas using a constant weight container or medium (filter paper, membrane) device, after evaporation, drying, and
constant weight. The gravimetric method was an early adopted method for determining oil content in water, and
there are still many people using the gravimetric method to determine water bodies with high oil content. When using
the gravimetric method, it is necessary to strictly control the dryness and wetness of the sampling tube, degreased
cotton quantitative filter paper, and the impact of dust contamination to prevent other oil pollution. During the sampling
and analysis process, no additional debris is allowed to adhere to the weighed container or medium. The balance weighing
must be rapid and accurate, as the mechanical and dust impurities in the air during sampling will affect the accuracy of oil
content. However, the low sensitivity of the gravimetric method determines that it is not suitable for accurately measuring
the oil content in gases, as the oil content in gases is quite low, and it is clearly not suitable to use the gravimetric method
for measurement.
2. Infrared spectrophotometry
Compressor oil contains oil substances with obvious absorption peaks in the infrared light region. After a certain volume of
liquid oxygen is naturally evaporated, the oil remains in the container. Dissolve the oil with tetrachloroethylene and bring to
volume. Using the Binci LS2600 infrared spectrophotometer (using infrared spectrophotometry) to determine the content
of oil in liquid oxygen, the accurate measurement of oil content concentration is closer to actual data, and the process operation
is very simple, accurate, and in line with industry standards.
Method 2: If the compressed gas does not have a liquid oil content, and the gas excluded from it can be added to a customized
filter cartridge management using special filter paper. After the filter cartridge pipeline, a flow valve is added to record the flow
rate, and a fixed solvent is used to clean the filter cotton to obtain near real oil content data.
3. UV spectrophotometry
The ultraviolet spectrophotometer (using ultraviolet spectrophotometry), due to its good * * * * degree and high sensitivity,
can measure trace amounts of oil in compressed gas. If the content is too high, it will exceed the limit detection value. It is
based on the characteristic absorption of aromatic compounds with conjugated bonds and benzene rings in the ultraviolet
region contained in the oil. Therefore, this method can be used to determine the concentration of oil in gas samples by measuring
the concentration of substances with conjugated double bond structures. This method is based on Lambert's law of light absorption.
Under the condition of pH ≤ 2, the oil substances in the product are extracted by n-hexane using an ultraviolet oil analyzer.
The extracted liquid is dehydrated by anhydrous sodium sulfate, and then adsorbed by magnesium silicate to remove polar
substances such as animal and plant oils. The absorbance is measured at a wavelength of 225 nm.
4. Chemical indicator tube method
The main manufacturers of instruments using the principle of chemical indicator tube method are Johnson Controls in the
United States and Delger in Germany. The oil content indicator of Johnson Controls is equipped with a gas detection agent,
which reacts with the oil to form a colored layer. Quantitative analysis is conducted based on the depth of the color layer or
the length of the color changing layer. Delge's oil detection method captures oil mist into the indicator layer of the oil detection
tube, and under the action of a catalyst, it produces black products with concentrated sulfuric acid in the oil detection tube. The
color depth is related to the oil content, and the oil content in the air is detected by colorimetry. This method generally only
determines whether the oil content is greater than a certain value and cannot obtain a specific value. This method is simple to
sample, but
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